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Reduction of the C–N triple bond to a double bond is confirmed on inspection of the bond length (C(27)–N(3) 1.292(4) Å), which is in line with average C N bond lengths. 36–39 Additionally, the change in angle around the nitrogen in XylNC from linear to bent (126.3 (2) °) confirms reduction of the C–N triple bond.

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Apr 04, 2020 · Monaco MR, Fazzi D, Tsuji N, Leutzsch M, Liao S, Thiel W, et al. The activation of carboxylic acids via self-assembly asymmetric organocatalysis: a combined experimental and computational investigation. J Am Chem Soc. 2016;138:14740–9. Crossref; PubMed
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